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Sodium Hydrogen Sulphate Solution (NaHSO4): Ions Present and pH

In general chemistry, what is a sodium hydrogen sulphate solution, what ions are present in water, and why is the solution acidic?

Subject: General Chemistry Chapter: Acid Base Equilibrium Topic: Hydrolysis Answer included
sodium hydrogen sulphate solution sodium bisulfate solution NaHSO4 hydrogen sulfate ion bisulfate acidic salt hydrolysis Ka2 sulfuric acid
Accepted answer Answer included

Chemical identity in water

A sodium hydrogen sulphate solution is an aqueous solution of sodium hydrogen sulfate, \(\mathrm{NaHSO_4}\). The name sodium bisulfate is commonly used for the same compound. In water, \(\mathrm{NaHSO_4}\) behaves as a strong electrolyte, so the ionic solute separates into ions:

\[ \mathrm{NaHSO_4(aq) \rightarrow Na^+(aq) + HSO_4^-(aq)} \]

The sodium ion \(\mathrm{Na^+}\) is a spectator ion in acid–base chemistry under typical conditions; the acid–base behavior comes from the hydrogen sulfate ion \(\mathrm{HSO_4^-}\).

Hydrogen sulfate \(\mathrm{HSO_4^-}\) is the conjugate base of a strong acid (\(\mathrm{H_2SO_4}\)) and still retains an acidic proton, so it can donate \(\mathrm{H^+}\) to water.

Acid–base equilibrium of \(\mathrm{HSO_4^-}\)

In water, \(\mathrm{HSO_4^-}\) acts as an acid and partially dissociates to sulfate:

\[ \mathrm{HSO_4^-(aq) + H_2O(l) \rightleftharpoons H_3O^+(aq) + SO_4^{2-}(aq)} \]

The equilibrium constant for this dissociation is often denoted \(\mathrm{K_a}\) for \(\mathrm{HSO_4^-}\) (equivalently \(\mathrm{K_{a2}}\) for sulfuric acid). At \(25^\circ\text{C}\), \(\mathrm{K_{a2}}\) is on the order of \(10^{-2}\), indicating a moderately strong weak-acid behavior.

pH of a sodium hydrogen sulphate solution

A quantitative pH estimate follows from the \(\mathrm{HSO_4^-}\) dissociation equilibrium. Consider an illustrative solution prepared with formal concentration \(C\) of \(\mathrm{NaHSO_4}\) at \(25^\circ\text{C}\). Strong-electrolyte dissociation gives an initial \(\mathrm{HSO_4^-}\) concentration approximately equal to \(C\).

Species Initial (M) Change (M) Equilibrium (M)
\(\mathrm{HSO_4^-}\) \(C\) \(-x\) \(C-x\)
\(\mathrm{H_3O^+}\) \(\approx 0\) \(+x\) \(x\)
\(\mathrm{SO_4^{2-}}\) \(\approx 0\) \(+x\) \(x\)

The equilibrium expression is

\[ K_a \;=\; \frac{[\mathrm{H_3O^+}][\mathrm{SO_4^{2-}}]}{[\mathrm{HSO_4^-}]} \;=\; \frac{x^2}{C-x} \]

Solving for \(x\) gives the hydronium concentration, \( [\mathrm{H_3O^+}] = x\), and the pH follows from

\[ \mathrm{pH} \;=\; -\log_{10}\!\big([\mathrm{H_3O^+}]\big) \;=\; -\log_{10}(x) \]

Worked numerical illustration

A concrete illustration uses \(C = 0.10\ \text{M}\) and a representative \(\mathrm{K_a} = 1.2\times 10^{-2}\) at \(25^\circ\text{C}\). The equilibrium condition becomes

\[ 1.2\times 10^{-2} \;=\; \frac{x^2}{0.10-x} \quad\Rightarrow\quad x^2 + (1.2\times 10^{-2})x - 1.2\times 10^{-3} = 0 \]

The physically meaningful root is

\[ x \;=\; \frac{-1.2\times 10^{-2} + \sqrt{(1.2\times 10^{-2})^2 + 4(1.2\times 10^{-3})}}{2} \;\approx\; 2.92\times 10^{-2}\ \text{M} \]

The corresponding pH is

\[ \mathrm{pH} \;\approx\; -\log_{10}(2.92\times 10^{-2}) \;\approx\; 1.53 \]

Speciation of sulfate in solution

The same \(x\) value provides a direct picture of sulfate speciation. For the example above, \([\mathrm{SO_4^{2-}}]=x\) and \([\mathrm{HSO_4^-}]=C-x\). The fraction as sulfate is \(x/C\), and the fraction remaining as hydrogen sulfate is \((C-x)/C\):

\[ \text{fraction as }\mathrm{SO_4^{2-}} = \frac{x}{C},\qquad \text{fraction as }\mathrm{HSO_4^-} = \frac{C-x}{C} \]

With \(C=0.10\ \text{M}\) and \(x\approx 2.92\times 10^{-2}\ \text{M}\), the distribution is about \(29\%\) \(\mathrm{SO_4^{2-}}\) and \(71\%\) \(\mathrm{HSO_4^-}\) (by concentration basis).

Visualization of species distribution

Speciation in sodium hydrogen sulphate solution Two vertical bars represent approximate fractions of HSO4- and SO4^2- for a 0.10 M NaHSO4 solution at 25 C, using Ka about 1.2e-2: about 71% HSO4- and 29% SO4^2-. 0 0.25 0.50 0.75 fraction of total sulfate species (example: \(C=0.10\ \text{M}\), \(25^\circ\text{C}\)) \(\mathrm{HSO_4^-}\) \(\mathrm{SO_4^{2-}}\) \(\approx 0.71\) \(\approx 0.29\)
The larger bar reflects the portion of sulfate present as \(\mathrm{HSO_4^-}\) in an aqueous sodium hydrogen sulphate solution; the smaller bar reflects \(\mathrm{SO_4^{2-}}\) formed by acid dissociation.

Common pitfalls

Sodium hydrogen sulfate is a salt, yet the solution is acidic because the anion \(\mathrm{HSO_4^-}\) contains a transferable proton and acts as an acid in water. Neutral salts (such as \(\mathrm{NaCl}\)) do not show this behavior because neither ion significantly reacts with water to generate \(\mathrm{H_3O^+}\) or \(\mathrm{OH^-}\).

The sodium ion \(\mathrm{Na^+}\) does not “create acidity” by itself; acidity is controlled by the \(\mathrm{HSO_4^- \rightleftharpoons SO_4^{2-}}\) equilibrium and the resulting hydronium concentration.

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